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Design of mixture experiments for the analysis of viscosity behavior of sulfonated polyacrylamide solutions (ATBS) with changes in salinity, hardness, and polymer concentration.
Diseño de experimentos de mezclas para el análisis del comportamiento de la viscosidad de soluciones de poliacrilamidas sulfonadas (ATBS) con cambios en la salinidad, dureza y concentración de polímero
DOI:
https://doi.org/10.15446/dyna.v89n221.100020Palabras clave:
ATBS; poliacrilamidas sulfonadas; salinidad; dureza; SCMD. (es)ATBS; sulfonated polyacrylamide; salinity; hardness; SCMD. (en)
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Un diseño de experimentos de mezcla (SCMD) fue usado para determinar el efecto de la dureza y salinidad del agua de preparación en la viscosidad final de una solución polimérica con modificaciones con unidades ATBS (Acrilamidas-Terbutil Sulfonadas). Con los resultados experimentales del SCMD se construyó un modelo cuadrático especial, y se implementó un modelo numérico que permite determinar la concentración de polímero necesaria para alcanzar la viscosidad deseada, dependiendo de la salinidad y dureza del agua de preparación. Adicionalmente, el modelo numérico desarrollado fue validado con datos experimentales de la literatura. Este puede predecir la concentración requerida de un polímero modificado con ATBS para alcanzar la viscosidad deseada con un 95% de confiabilidad en los rangos evaluados. El modelo numérico de Newton-Raphson desarrollado usando un SCMD es el primero reportado en la literatura que permite determinar la concentración de polímeros ATBS necesaria para conocer un rango de viscosidad.
A simple centroid mixture design (SCMD) method was used to determine the effect of the preparation water’s salinity and hardness on the polymers modified with Acrylamide-Tert-butyl-Sulfonated units (ATBS) solution's final viscosity. With the experimental results of SCMD, a special quartic model was carried out, and a numerical model was implemented that allows determining the concentration of polymer necessary to reach the desired viscosity, depending on the salinity and hardness of the preparation water. In addition, the numerical model developed was validated with experimental data from the literature. It could predict the required concentration of a modified polymer (ATBS) to achieve the desired injection viscosity of the polymeric solution with 95% reliability in the ranges evaluated. The Newton-Raphson numerical model developed using an SMCD is the first reported in the literature that allows determining the concentration of ATBS polymer necessary to know the viscosity range
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1. Eduar Pérez, Dario Alviso, Mauricio Carmona, Eduardo Manrique, Guillermo Artana. (2024). A simple model of the rheological curve of HPAM solutions at different temperatures. Scientific Reports, 14(1) https://doi.org/10.1038/s41598-024-79242-0.
2. Eduar Pérez, Dario Alviso, Horacio Burbridge, Vladimir Alvarado, Eduardo Manrique, Guillermo Artana. (2025). Rapid Rheogram Prediction for Mechanically Degraded Hydrolyzed Polyacrylamide Solutions via Standard Viscosity Measurements. SPE Journal, 30(11), p.7097. https://doi.org/10.2118/230289-PA.
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