Publicado

2018-01-01

Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template

Síntesis hidrotermal de nanobarras de hidroxiapatita usando plantillas de extractos de fruta

DOI:

https://doi.org/10.15446/dyna.v85n204.65773

Palabras clave:

hydroxyapatite, bioceramics, nanorods, hydrothermal reaction, fruit extract template (en)
hidroxiapatita, biocerámicos, nanobarras, síntesis hidrotermal, plantilla de extracto de fruta (es)

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Biocompatible materials development for the replacement of human body parts has been one of the needs of science. Hydroxyapatite is a bioceramic similar to the mineral component present in the human hard tissues and animal body. In this work, hydroxyapatite nanorods were synthesized and characterized using a hydrothermal reaction with templates of fruit extracts in order to control the particles size and morphology. The powders obtained were characterized by scanning electron microscopy, X-ray diffraction, and infrared spectroscopy. Hydroxyapatite nanorods were obtained with diameters between 43.47 and 48.56 nm and lengths between 148.47 and 265.96 nm. For all assays, an adequate HA synthesis was confirmed because the XRD showed the main and secondary peaks. The crystallite size was calculated with the Scherrer equation, obtaining values between 5.99 and 6.96 nm and percentages crystallinity between 55.61 and 65.9%. The synthesized material can be a suitable biomaterial for the manufacture of bone substitutes.
El desarrollo de biomateriales para el reemplazo de partes del cuerpo humano ha sido una de las necesidades de la ciencia. La hidroxiapatita es un biocerámico similar al componente mineral de los tejidos duros del cuerpo humano y animal. En la presente investigación se sintetizaron nanobarras de hidroxiapatita usando síntesis hidrotermal con plantillas de extractos de fruta para controlar el tamaño de partícula, los polvos obtenidos se caracterizaron por microscopia electrónica de barrido, difracción de rayos x y espectroscopia infrarroja. Las nanobarras obtenidas presentaron diámetros entre 43,47 y 48,56 nm, longitudes entre 148,47 y 265,96 nm, para todos los ensayos los DRX mostraron los picos principales y secundarios de la hidroxiapatita. El tamaño del cristalito fue calculado con la ecuación de Scherrer con valores entre 5,99 y 6,96 nm y porcentajes de cristalinidad entre 55,61 y 65,9%. En conclusión el material sintetizado puede usarse como biomaterial para aplicaciones óseas.

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