Published

2022-01-01

Selecting optimal parameters for obtaining the extract of red grape pomace

Selección de parámetros óptimos para la obtención de extracto de uva roja

DOI:

https://doi.org/10.15446/rfnam.v75n1.94175

Keywords:

Extraction Regimen, Flavonoids, Anthocyanins, Antioxidative Activity, Grape Pomace (en)
Régimen de extracción, flavonoides, antocianinas, actividad antioxidante, hollejo, bagazo (es)

Downloads

Authors

Due to the industrial processing of grapes, large amounts of by-products are produced. The main varieties of by-products are pomace, which is comprised of skins, seeds and any other solid remaining after pressing process and sediments. It is necessary to implement new effective ways of processing to minimize these residues. This problem is relevant for all the wine-producing countries, including Georgia. It is well-known fact that pomace is an important source of phenolic compounds, which are characterized by high antioxidant activity and possess healing-prophylactic properties. It is also worth mentioning that pomace is an easily spoiled product, and without the proper processing, it cannot be stored for a long time. Thus, this research aimed to obtain optimal parameters for extraction, preserving the antioxidant characteristics. The optimal range of the following parameters for extraction was determined: the temperature for drying 45-50 °C, grinding level 1.5 mm, diluent concentration 70% ethanol/water solvent, extraction module 1:20, extraction temperature 50-55 °C, and duration 2 h. This determination of technological parameters of extraction was done according to the best physical-chemical measures and antioxidant activity level. The physical-chemical tests were performed according to the European Union standards. These parameters can produce an extract with distinct antioxidant characteristics that can be used in the food industry as a natural antioxidant. The extract with distinct antioxidant properties was obtained, which can be used in the food industry as a natural antioxidant.

Debido al procesamiento industrial de la uva, se producen grandes cantidades de subproductos. Las principales variedades de subproductos son el orujo, que se compone de cáscara, semillas y cualquier otro sólido que quede después del proceso de prensado y sedimentos. Es necesario implementar nuevas formas efectivas de procesamiento para minimizar estos residuos. Este problema es relevante para todos los países productores de vino, incluido Georgia. Es bien sabido que el orujo es una fuente importante de compuestos fenólicos, que se caracterizan por una alta actividad antioxidante y poseen propiedades curativas profilácticas. También vale la pena mencionar que el orujo es un producto que se estropea fácilmente y, sin el procesamiento adecuado, no se puede almacenar durante mucho tiempo. Por lo tanto, esta investigación tuvo como objetivo obtener los parámetros óptimos de extracción, conservando las características antioxidantes. Se determinó el rango óptimo  de los siguientes parámetros para la extracción: temperatura de secado 45-50 °C, nivel de molienda 1,5 mm, concentración de diluyente 70% etanol/agua solvente, módulo de extracción 1:20, temperatura de extracción 50 55 °C y duración 2 h. Esta determinación de los parámetros tecnológicos de extracción se realizó de acuerdo con las mejores medidas físico-químicas y nivel de actividad antioxidante. Las pruebas físico-químicas se realizaron de acuerdo con los estándares de la Unión Europea. Se obtuvo un extracto con altas propiedades antioxidantes, que puede ser utilizado en la industria alimentaria como antioxidante natural.

References

Amendola D, De Faveri DM and Spigno G. 2010. Grape marc phenolics: Extraction kinetics, quality and stability of extracts. Journal of Food Engineering 97(3): 384–392. https://doi.org/10.1016/j.jfoodeng.2009.10.033

Atta EM, Mohamed NH and Abdelgawad AAM. 2017. Antioxidants: An overview on the natural and synthetic types. European Chemical Bulletin 6(8): 365-375. https://doi.org/10.17628/ecb.2017.6.374-384

Brewer LR, Kubola J, Siriamornpun S, Herald TJ and Shi YC. 2013. Wheat bran particle size influence on phytochemical extractability and antioxidant properties. Food Chemistry 152: 483-490. https://doi.org/10.1016/j.foodchem.2013.11.128

Carmona-Jiménez Y, García-Moreno MV and García-Barroso C. 2018. Effect of drying on the phenolic content and antioxidant activity of red grape pomace. Plant Foods for Nutrition 73(1): 74-81. https://doi.org/10.1007/s11130-018-0658-1

Charalampia D and Koutekidakis A. 2016. Grape pomace: a challenging renewable resource of bioactive phenolic compounds with diversified health benefits. Food Processing & Technology 3(1): 262-265. https://doi.org/10.15406/mojfpt.2016.03.00065

Dimcheva V, Karsheva M, Diankov S and Hinkov I. 2018. Optimization of extraction of antioxidants from Bulgarian Mavrud By-Products. Journal of Chemical Technology and Metallurgy 53(4): 631-639.

García-Lomillo J and González-SanJosé ML. 2016. Applications of wine pomace in the food industry: Approaches and functions. Comprehensive Reviews in Food Science and Food Safety 16(1): 3-22. https://doi.org/10.1111/1541-4337.12238

Goula A, Thymiatis K and Kaderides K. 2016. Valorization of grape pomace: Drying behavior and ultrasound extraction of phenolics. Food and Bioproducts Processing 100: 132-144. https://doi.org/10.1016/j.fbp.2016.06.016

Iuga M and Mironeasa S. 2020. Potential of grape byproducts as functional ingredients in baked goods and pasta. Comprehensive Reviews in Food Science and Food Safety 19(5): 2473-2505. https://doi.org/10.1111/1541-4337.12597

Jelley R. E, Herbst-Johnstone M, Klaere S, Pilkington L. I, Grose C, Martin D, Barker D and Fedrizzi B. 2016. Optimization of ecofriendly extraction of bioactive monomeric phenolics and useful flavor precursors from grape waste. ACS Sustainable Chemistry & Engineering 4(9): 5060-5067. https://doi.org/10.1021/acssuschemeng.6b01551

Ju ZY and Hovard LR. 2003. Effect of solvent and temperature on pressurized liquid extraction of anthocyanins and total phenolics from dried red grape skin. Journal of Agricultural and Food Chemistry 51(18): 5207–5213. https://doi.org/10.1021/jf0302106

Kedare SB and Singh RP. 2011. Genesis and development of DPPH method of antioxidant assay. Journal of Food Science and Technology 48(4): 412-422. https://doi.org/10.1007/s13197-011-0251-1

Khanal RC, Howard L and Prior RL. 2010. Effect of heating on the stability of grape and blueberry pomace procyanidins and total anthocyanins. Food research international 43(5): 1464-1469. https://doi.org/10.1016/j.foodres.2010.04.018

Knorr D, Augustin M. A and Tiwari B. 2020. Advancing the role of food processing for improved integration in sustainable food chains. Frontiers in Nutrition 7: 34. https://doi.org/10.3389/fnut.2020.00034

Kurozawa LM, Terng I, Hubinger MD and Park KJ. 2014. Ascorbic acid degradation of papaya during drying: Effect of process conditions and glass transition phenomenon. Journal of Food Engineering 123: 157–164. https://doi.org/10.1016/j.jfoodeng.2013.08.039

Li S, Chen G, Zhang CH, Wu M, Wu Sh and Liu Q. 2014. Research progress of natural antioxidants in foods for the treatments of diseases. Food Science and Human Wellness 3: 110-116. https://doi.org/10.1016/j.fshw.2014.11.002

Lin YC and Chou CC. 2008. Effect of heat treatment on total phenolic and anthocyanin contents as well as antioxidant activity of the extract from Aspergillus awamori-fermented black soybeans, a healthy food ingredient. International Journal of Food Science and Nutrition 60(7): 627-36. https://doi.org/10.3109/09637480801992492

Luchian CE, Cotea VV, Vlase L, Toiu AM, Colibaba LC, Răschip IE, Nadăş G, Gheldiu, C. Tuchiluş AM and Rotaru L. 2019. Antioxidant and antimicrobial effect of grape pomace extracts. BIO Web of Conferences 15. 42nd World Congress of Vine and Wine. https://doi.org/10.1051/bioconf/20191504006

Mitterer-Daltoe M, Bordim J, Lise C, Breda L, Casagrande M and Lima V. 2020. Consumer awareness of food antioxidants. Synthetic vs. Natural. Food Science and Technology 41 Supp. 1: 208-212. https://doi.org/10.1590/fst.15120

Pazir F, Koçak E, Turan F and Ova G. 2020. Extraction of anthocyanins from grape pomace by using supercritical carbon dioxide. Journal of Food Processing and Preservation 45(8): e14950 Special Issue: AgroFood Conference, Turkey. https://doi.org/10.1111/jfpp.14950

Raiba HN, El Darra Z, Hobaika Z, Bousseta N, Vorobiev E, Maroun RG and Louka N. 2014. Extraction of total phenolic compounds, flavonoids, anthocyanins and tannins from grape byproducts by response surface methodology. Influence of solidliquid ratio, particle size, time, temperature and solvent mixtures on the optimization process. Food and Nutrition Science 5(4): 397-409. https://doi.org/10.4236/fns.2014.54048

Teixeira A, Baenas N, Dominguez-Perles R, Barros A, Rosa E, Moreno D. A and Garcia-Viguera C. 2014. Natural bioactive compounds from winery by-products as health promoters: A Review. International Journal of Molecular Sciences 15(9): 15638–15678. https://doi.org/10.3390/ijms150915638

Yilmaz Y and Toledo RT. 2006. Oxygen radical absorbance capacities of grape/wine industry byproducts and effect of solvent type on extraction of grape seed polyphenols. Journal of Food Composition and Analysis 19(1): 41–48. https://doi.org/10.1016/j.jfca.2004.10.009

How to Cite

APA

Gurgenidze, L., Kanchaveli, T. . & Kvartskhava, G. . (2022). Selecting optimal parameters for obtaining the extract of red grape pomace. Revista Facultad Nacional de Agronomía Medellín, 75(1), 9831–9837. https://doi.org/10.15446/rfnam.v75n1.94175

ACM

[1]
Gurgenidze, L., Kanchaveli, T. and Kvartskhava, G. 2022. Selecting optimal parameters for obtaining the extract of red grape pomace. Revista Facultad Nacional de Agronomía Medellín. 75, 1 (Jan. 2022), 9831–9837. DOI:https://doi.org/10.15446/rfnam.v75n1.94175.

ACS

(1)
Gurgenidze, L.; Kanchaveli, T. .; Kvartskhava, G. . Selecting optimal parameters for obtaining the extract of red grape pomace. Rev. Fac. Nac. Agron. Medellín 2022, 75, 9831-9837.

ABNT

GURGENIDZE, L.; KANCHAVELI, T. .; KVARTSKHAVA, G. . Selecting optimal parameters for obtaining the extract of red grape pomace. Revista Facultad Nacional de Agronomía Medellín, [S. l.], v. 75, n. 1, p. 9831–9837, 2022. DOI: 10.15446/rfnam.v75n1.94175. Disponível em: https://revistas.unal.edu.co/index.php/refame/article/view/94175. Acesso em: 22 mar. 2026.

Chicago

Gurgenidze, Lela, Tamar Kanchaveli, and Giorgi Kvartskhava. 2022. “Selecting optimal parameters for obtaining the extract of red grape pomace”. Revista Facultad Nacional De Agronomía Medellín 75 (1):9831-37. https://doi.org/10.15446/rfnam.v75n1.94175.

Harvard

Gurgenidze, L., Kanchaveli, T. . and Kvartskhava, G. . (2022) “Selecting optimal parameters for obtaining the extract of red grape pomace”, Revista Facultad Nacional de Agronomía Medellín, 75(1), pp. 9831–9837. doi: 10.15446/rfnam.v75n1.94175.

IEEE

[1]
L. Gurgenidze, T. . Kanchaveli, and G. . Kvartskhava, “Selecting optimal parameters for obtaining the extract of red grape pomace”, Rev. Fac. Nac. Agron. Medellín, vol. 75, no. 1, pp. 9831–9837, Jan. 2022.

MLA

Gurgenidze, L., T. . Kanchaveli, and G. . Kvartskhava. “Selecting optimal parameters for obtaining the extract of red grape pomace”. Revista Facultad Nacional de Agronomía Medellín, vol. 75, no. 1, Jan. 2022, pp. 9831-7, doi:10.15446/rfnam.v75n1.94175.

Turabian

Gurgenidze, Lela, Tamar Kanchaveli, and Giorgi Kvartskhava. “Selecting optimal parameters for obtaining the extract of red grape pomace”. Revista Facultad Nacional de Agronomía Medellín 75, no. 1 (January 1, 2022): 9831–9837. Accessed March 22, 2026. https://revistas.unal.edu.co/index.php/refame/article/view/94175.

Vancouver

1.
Gurgenidze L, Kanchaveli T, Kvartskhava G. Selecting optimal parameters for obtaining the extract of red grape pomace. Rev. Fac. Nac. Agron. Medellín [Internet]. 2022 Jan. 1 [cited 2026 Mar. 22];75(1):9831-7. Available from: https://revistas.unal.edu.co/index.php/refame/article/view/94175

Download Citation

CrossRef Cited-by

CrossRef citations4

1. Vincenzo Roselli, Rosalba Leuci, Gianluca Pugliese, Alexia Barbarossa, Antonio Laghezza, Marco Paparella, Alessia Carocci, Vincenzo Tufarelli, Lucia Gambacorta, Luca Piemontese. (2025). Deep Eutectic Solvents (DESs) as Alternative Sustainable Media for the Extraction and Characterization of Bioactive Compounds from Winemaking Industry Wastes. Molecules, 30(8), p.1855. https://doi.org/10.3390/molecules30081855.

2. Petronela Anca Onache, Elisabeta-Irina Geana, Corina Teodora Ciucure, Alina Florea, Dorin Ioan Sumedrea, Roxana Elena Ionete, Ovidiu Tița. (2022). Bioactive Phytochemical Composition of Grape Pomace Resulted from Different White and Red Grape Cultivars. Separations, 9(12), p.395. https://doi.org/10.3390/separations9120395.

3. Eva Ccacyancco-Cáceres, Guido Sarmiento-Sarmiento, Laydy Mena-Chacón. (2024). Use of processed grape pomace and whey bio ferment to improve the agronomic performance of radish (Raphanus sativus L.) in arid soils. Revista Facultad Nacional de Agronomía Medellín, 77(2), p.10707. https://doi.org/10.15446/rfnam.v77n2.109370.

4. Teresa Abreu, Catarina Luís, José S. Câmara, Juan Teixeira, Rosa Perestrelo. (2025). Unveiling potential functional applications of grape pomace extracts based on their phenolic profiling, bioactivities, and circular bioeconomy. Biomass Conversion and Biorefinery, 15(24), p.31491. https://doi.org/10.1007/s13399-025-06578-6.

Dimensions

PlumX

Article abstract page views

599

Downloads

Download data is not yet available.